Experimental Organic Chemistry: A Miniscale and Microscale Approach , Fifth Edition (Brooks Cole Laboratory Series for Organic Chemistry)
by: John C. Gilbert, Stephen F. Martin
year: 2010
pages: 966
description: ( ? )
Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as all scale) and microscale users. The manual first provides an early focus on equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and yze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide.
Contents
1. Introduction, Record Keeping, and Laboratory Safety.
2. Techniques and Apparatus.
3. Solids: Recrystallization and Melting Points.
4. Liquids: Distillation and Boiling Points.
5. Extraction.
6. Chromatography.
7. Stereoisomers.
8. Spectral Methods.
9. Alkanes.
10. Alkenes.
11. Alkynes.
12. Dienes: The Diels-Alder Reaction.
13. Kinetic and Thermodynamic Control of a Reaction.
14. Nucleophilic Aliphatic Substitution: Preparation for Alkyl Halides.
15. Electrophilic Aromatic Substitution.
16. Oxidation of Alcohols and Carbonyl Compounds.
17. Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines.
18. Reactions of Carbonyl Compounds.
19. Organometallic Chemistry.
20. Carboxylic Acids and Their Derivatives.
21. Multistep Organic Synthesis.
22. Polymers.
23. Carbohydrates.
24. Amino Acids and Peptides.
25. Identifying Organic Compounds.
26. The Literature of Organic Chemistry.
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